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Chemical structures of glyphosate, N -acetyl glyphosate, glufosinate, N -acetyl glufosinate, and MPPA.

Journal: Food Chemistry: X

Article Title: Simultaneous determination of glyphosate, glufosinate and their metabolites in soybeans using solid-phase analytical derivatization and LC-MS/MS determination

doi: 10.1016/j.fochx.2024.101806

Figure Lengend Snippet: Chemical structures of glyphosate, N -acetyl glyphosate, glufosinate, N -acetyl glufosinate, and MPPA.

Article Snippet: Standard reagent grade glyphosate, glufosinate ammonium, and MPPA were purchased from FUJIFILM Wako Pure Chemicals Co. (Osaka, Japan).

Techniques:

MRM chromatograms of (a) standard solution, (b) soybean blank, and (c) spiked soybeans. (a) Standard solutions were adjusted to 0.5 μg/L for glyphosate (−tri t BDMS) and Gly-A (−tri t BDMS), and to 0.05 μg/L for glufosinate (−di t BDMS), Glu-A (−di t BDMS), and MPPA (−di t BDMS). (c) Spiked soybean samples were spiked at 5 mg/kg for glyphosate (−tri t BDMS) and Gly-A (−tri t BDMS), and at 0.5 mg/kg for glufosinate (−di t BDMS), Glu-A (−di t BDMS), and MPPA (−di t BDMS).

Journal: Food Chemistry: X

Article Title: Simultaneous determination of glyphosate, glufosinate and their metabolites in soybeans using solid-phase analytical derivatization and LC-MS/MS determination

doi: 10.1016/j.fochx.2024.101806

Figure Lengend Snippet: MRM chromatograms of (a) standard solution, (b) soybean blank, and (c) spiked soybeans. (a) Standard solutions were adjusted to 0.5 μg/L for glyphosate (−tri t BDMS) and Gly-A (−tri t BDMS), and to 0.05 μg/L for glufosinate (−di t BDMS), Glu-A (−di t BDMS), and MPPA (−di t BDMS). (c) Spiked soybean samples were spiked at 5 mg/kg for glyphosate (−tri t BDMS) and Gly-A (−tri t BDMS), and at 0.5 mg/kg for glufosinate (−di t BDMS), Glu-A (−di t BDMS), and MPPA (−di t BDMS).

Article Snippet: Standard reagent grade glyphosate, glufosinate ammonium, and MPPA were purchased from FUJIFILM Wako Pure Chemicals Co. (Osaka, Japan).

Techniques:

Validation results in soybeans spiked Glyphosate, Gly-A, Glufosinate, Glu-A and MPPA.

Journal: Food Chemistry: X

Article Title: Simultaneous determination of glyphosate, glufosinate and their metabolites in soybeans using solid-phase analytical derivatization and LC-MS/MS determination

doi: 10.1016/j.fochx.2024.101806

Figure Lengend Snippet: Validation results in soybeans spiked Glyphosate, Gly-A, Glufosinate, Glu-A and MPPA.

Article Snippet: Standard reagent grade glyphosate, glufosinate ammonium, and MPPA were purchased from FUJIFILM Wako Pure Chemicals Co. (Osaka, Japan).

Techniques: Biomarker Discovery

Analytical results of distributed edible soybeans in Japan.

Journal: Food Chemistry: X

Article Title: Simultaneous determination of glyphosate, glufosinate and their metabolites in soybeans using solid-phase analytical derivatization and LC-MS/MS determination

doi: 10.1016/j.fochx.2024.101806

Figure Lengend Snippet: Analytical results of distributed edible soybeans in Japan.

Article Snippet: Standard reagent grade glyphosate, glufosinate ammonium, and MPPA were purchased from FUJIFILM Wako Pure Chemicals Co. (Osaka, Japan).

Techniques:

Analytical results of feed-use soybean and soybean meal (mg/kg).

Journal: Food Chemistry: X

Article Title: Simultaneous determination of glyphosate, glufosinate and their metabolites in soybeans using solid-phase analytical derivatization and LC-MS/MS determination

doi: 10.1016/j.fochx.2024.101806

Figure Lengend Snippet: Analytical results of feed-use soybean and soybean meal (mg/kg).

Article Snippet: Standard reagent grade glyphosate, glufosinate ammonium, and MPPA were purchased from FUJIFILM Wako Pure Chemicals Co. (Osaka, Japan).

Techniques: